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IJSTR >> Volume 1 - Issue 1, February 2012 Edition



International Journal of Scientific & Technology Research  
International Journal of Scientific & Technology Research

Website: http://www.ijstr.org

ISSN 2277-8616



Synthesis and Characterisation of Two Random Copolyesters by Phase Transfer Catalysed Polycondensation

[Full Text]

 

AUTHOR(S)

R.Senthamizh Selvi

 

KEYWORDS

Copolyesters; spectral studies; phase-transfer catalyst; polycondensation

 

ABSTRACT

Polyesters containing chalcone moiety were synthesised from 1, 3-bis (4-hydroxy-3-methoxyphenyl) propenone (BHMPP) and 1- (3, 5-dihydroxyphenyl)-3-(4-methoxyphenyl) propenone (DHPMPP) with suberoyl and sebacoyl chlorides by an interfacial polycondensation technique. Fundamental studies on the two phase polycondensation using phase transfer catalyst (tetra n-butylammonium bromide) was done. The synthesised polymers were characterised by solubility measurement, intrinsic viscosity, IR, 1H and 13C NMR studies. Keywords:Copolyesters; spectral studies; phase-transfer catalyst; polycondensation

 

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